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Clustering of Tadalafil API Samples According to their Manufacturer in the Context of API Falsification Detection
falsified samples. In total, 46 tadalafil API samples from 13 different manufacturers were collected. For all samples fingerprint data was collected through analysis of impurities and residual solvents, mass ...
Multidimensional Fingerprint Development for the Detection of Tribulus terrestris in Plant Food Supplements
by the ease with which they can be purchased from various illegal channels, necessitating an efficient screening approach. This study aims to develop a multidimensional approach using chromatographic ...
CHROMATOGRAPHIC FINGERPRINT DEVELOPMENT FOR THE DETECTION OF TRIBULUS TERRESTRIS IN PLANT FOOD SUPPLEMENTS
by preparing triturations of TT with herbal matrices in varying ratios (½, ⅕, 1/10, 1/15, ½0). Twenty unknown samples were screened for TT and further confirmation was carried out by UH ¨ PLC-mass ...
The occurrence of putative cognitive enhancing research peptides in seized pharmaceutical preparations: An incentive for controlling agencies to prepare for future encounters of the kind.
recommendation paper of the General European Official Medicines Control Laboratory (OMCL) network on the interpretation of screening results for unknown peptides by mass spectrometry, was also validated in ...
Development and validation of chromatographic methods for screening and subsequent quantification of suspected illegal antimicrobial drugs encountered on the Belgian market.
a screening and a quantification method using ultra-high performance liquid chromatography with tandem mass spectrometry (UHPLC- MS) and diode array detection (UHPLC- DAD), respectively were developed and ...
Analysis of illegal peptide drugs via HILIC-DAD-MS.
five different HILIC columns were selected and screened for their chromatographic performance. Among those columns, the ZIC HILIC column showed the best performance under the tested screening conditions ...
A simple dilute and shoot methodology for the identification and quantification of illegal insulin
Number 334, p.326- 334 (2016) Keywords: illegal insulin LC–DAD–MS/MS Quantification method Screening method Abstract: The occurrence of illegal medicines is a well-established global problem and concerns ...