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Development and validation of chromatographic methods for screening and subsequent quantification of suspected illegal antimicrobial drugs encountered on the Belgian market.

a screening and a quantification method using ultra-high performance liquid chromatography with tandem mass spectrometry (UHPLC- MS) and diode array detection (UHPLC- DAD), respectively were developed and ...

Monitoring of pyrrolizidine alkaloids in beehive products and derivatives on the Belgian market

(2019) Keywords: Beehive products Candies Food Supplements pollen Pyrrolizidine alkaloids UHPLC-MS/MS Honey Belgium Snacks Abstract: Pyrrolizidine alkaloids (PA s) and related N-oxides (PANO s) are ...

Development of a QuEChERS-Based UHPLC-MS/MS Method for Simultaneous Determination of Six Alternaria Toxins in Grapes

Han, Zheng Source: Toxins, Volume 11, Issue 2, Number 100 (2019) Keywords: Alternaria toxins Grape modified QuEChERS UHPLC-MS/MS Abstract: A simple and reliable analytical method for the simultaneous ...

Towards the use of ion mobility mass spectrometry derived collision cross section as a screening approach for unambiguous identification of targeted pesticides in food

(IMS ‐ MS). Methods All experiments were carried out using UHPLC coupled to a travelling wave ion mobility mass spectrometer equipped with an electrospray ionization (ESI) source working in positive ...

Development and validation of chromatographic methods for screening and subsequent quantification of suspected illegal antimicrobial drugs encountered on the Belgian market

antimicrobials UHPLC-DAD UHPLC-MS2 Abstract: Estimations, made by the World Health Organization (WHO), state that 10% of the medical products in low- and middle-income countries are substandard or falsified (SF). ...

Development and validation of a quantitative UHPLC-MS/MS method for selected brominated flame retardants in food.

Joris Van Loco Source: Food Addit Contam Part A Chem Anal Control Expo Risk Assess (2017) Keywords: brominated flame retardants bromophenols Food Analysis HBCDsTBBPA UHPLC-MS/MS Abstract: An ultra-high ...

Detection of pyrrolizidine alkaloids in milk and honey on the Belgian market using UHPLC-MS/MS.

public Pyrrolizidine alkaloids report Research result results SAFETY Sample Samples sampling SENSITIVITY separation Service Tea toxin UHPLC-MS/MS UPLC VALIDATION variety world Abstract: The objective of ...

Analysis of illegal peptide biopharmaceuticals frequently encountered by controlling agencies.

diode array detection (UHPLC- DAD). The screening method, taking only 30 min, is able to selectively detect 25 different peptides and incorporates the proposed minimum of five identification points (IP) ...

Determination of selected veterinary antimicrobials in poultry excreta by UHPLC-MS/MS, for application in Salmonella control programs.

zoonotic Salmonella spp. To uncover illicit use, an analytical method using ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC- MS / MS) for the determination of antimicrobial ...

Development and validation of an ultra-high performance liquid chromatography-tandem mass spectrometry method to measure creatinine in human urine.

spectrometry (UHPLC- MS / MS) method was developed to measure creatinine in small volumes of human urine. In this method, urine samples are simply diluted with a basic mobile phase and injected directly under ...

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