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Development of a QuEChERS-Based UHPLC-MS/MS Method for Simultaneous Determination of Six Alternaria Toxins in Grapes

chromatography–tandem mass spectrometry (UHPLC- MS / MS). A modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) procedure with the extraction by acetonitrile and purification by sodium chloride (0.5 g) ...

Dietary exposure to pyrrolizidine alkaloids in young children and adults from the Belgian population (PASFOOD)

methods was required to detect the presence of PA s at ppb or even ppt levels.   Analytical methods based on analytes extraction and SPE purification, followed by UPLC separation and MS / MS detection were ...

Detection of pyrrolizidine alkaloids in milk and honey on the Belgian market using UHPLC-MS/MS.

The sample preparation involves acidic extraction of the analytes followed by SCX- SPE purification to avoid loss of sensitivity due to matrix effect. Several parameters were optimized in order to ...

Scalable chromatography-based purification of virus-like particle carrier for epitope based influenza A vaccine produced in Escherichia coli.

downstream processes. In particular, a rapid low cost purification process has been identified as a remaining key challenge in manufacturing process development. In the present study we set up a size-exclusion ...

Development and validation of an ultra-high performance liquid chromatography-tandem mass spectrometry method to measure creatinine in human urine.

positive electrospray ionization (ESI) conditions, without further purification steps. The combination of an important diluting factor (10(4) times) due to the use of a very sensitive triple quadrupole mass ...

Revisiting susceptibility testing in MDR-TB by a standardized quantitative phenotypic assessment in a European multicentre study9

European EVALUATION France gene genetics Genotype Genotyping Techniques Germany growth & development health Help Humans im Impact Infectious Infectious diseases Institute IS isolation & purification ...

Evolutionary history and global spread of the Mycobacterium tuberculosis Beijing lineage20

immunology Increase Increases INFECTION Infectious Infectious diseases Institute International IS isolation & purification IT ITALY Japan journal Laboratories london Lung Lung Diseases Maryland medical ...

Start of the 2014/15 influenza season in Europe: drifted influenza A(H3N2) viruses circulate as dominant subtype36933

purification journal middle aged Phylogeny prevention SB- IM Seasons Sentinel Surveillance statistics & numerical data Sweden virology Viruses Young adult Abstract: NA Service:  Virale ziekten Viral diseases ...

Systematic identification of hypothetical bacteriophage proteins targeting key protein complexes of pseudomonas aeruginosa

Using affinity purifications of these host protein complexes coupled to mass spectrometric analyses, 37 host complex-associated phage proteins could be identified. Importantly, eight of these show an ...

Proteomic detection as an alternative for the quantification of Staphylococcus aureus enterotoxins

identification identify Immunoassay IS matrix Meat method methods microorganism milk ON outbreak Peptides poisoning prevention PROCESSES protein purification Quantification RANGE Sample Samples Selection specific ...

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