Search results - 201 results

Validation of a Targeted LC-MS/MS Method for Cereulide and Application in Food and Faeces.

food. This work aimed to develop and validate a targeted analytical method applying liquid chromatography-tandem mass spectrometry (LC- MS / MS) to quantify this toxin in food and human faeces. Samples ...

Development, validation, and application of a multimatrix UHPLC-MS/MS method for quantification of Datura-type alkaloids in food

spectrometry (UHPLC- MS / MS) method was developed and validated for the determination of tropane alkaloids (TA s), atropine and scopolamine, in a variety of food products. The sample preparation of cereal-based ...

Applicability of the DPRA on mixture testing: challenges and opportunities.

Keywords: Animal Testing Alternatives Animals Peptides Abstract: The in chemico direct peptide reactivity assay (DPRA) is validated to assess protein reactivity of chemical compounds, relating to the ...

The analysis of cannabinoids in e-cigarette liquids using LC-HRAM-MS and LC-UV.

available to the Belgian population, a method was developed for screening of 17 cannabinoids and to quantify the major cannabinoids such as CBD, CBDA, ∆9- THC and ∆9- THCA. The latter was fully validated ...

Occurrence of microcystin congeners in surface waters and food in Belgium as a source of exposure to humans

group worldwide, the microcystin congeners (MC s). After method validation, the quantitative UHPLC- MS / MS approaches were applied to Belgian samples to characterize potential human exposure sources in ...

Multidimensional Chromatographic Fingerprinting Combined with Chemometrics for the Identification of Regulated Plants in Suspicious Plant Food Supplements.

the approach not so straightforward. This paper aims to tackle this problem by developing a multidimensional chromatographic fingerprinting method aided by chemometrics. To render more specificity to ...

The analysis of cannabinoids in e-cigarette liquids using LC-HRAM-MS and LC-UV

a method was developed for screening of 17 cannabinoids and to quantify the major cannabinoids such as CBD, CBDA, ∆9- THC and ∆9- THCA. The latter was fully validated using the ‘total error’ approach, ...

Using random-forest multiple imputation to address bias of self-reported anthropometric measures, hypertension and hypercholesterolemia in the Belgian health interview survey

height, weight, hypertension and hypercholesterolemia and to identify an adequate approach for valid measurement error correction. METHODS: Nine thousand four hundred thirty-nine participants of the 2018 ...

Development of a Droplet Digital PCR to Monitor SARS-CoV-2 Omicron Variant BA.2 in Wastewater Samples

applicability of the proposed RT-ddPCR method was evaluated to monitor and quantify the emergence of the BA.2 variant over time. To validate this assay as a proof of concept, the measurement of the proportion of ...

Development, validation, and application of a multimatrix UHPLC-MS/MS method for quantification of Datura-type alkaloids in food

Volume 40, Issue 10 (2023) Keywords: food Food Supplements LC-MS/MS tropane alkaloids VALIDATION Health Topics:  Food consumption and food safety Consommation et sécurité alimentaires Voedselconsumptie en ...

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